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Evaluation of fracture toughness of ZrO2 and Si3N4 engineering ceramics following CO2 and fibre laser surface treatment

机译:CO2和光纤激光表面处理后ZrO2和Si3N4工程陶瓷的断裂韧性评估

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摘要

The fracture toughness property (K1c) of Si3N4 and ZrO2 engineering ceramics was investigated by means of CO2 and a fibre laser surface treatment. Near surface modifications in the hardness was investigated by employing the Vickers indentation method. Crack lengths and geometry were then measured by using the optical. A co-ordinate measuring machine was used to investigate the diamond indentations and to measure the lengths of the cracks. Thereafter, computational and analytical methods were employed to determine the K1C. An increase in the K1C of both ceramics was found by the CO2 and the fibre laser surface treatment in comparison to the as-received surfaces. The K1C of the CO2 laser radiated surface of the Si3N4 was over 3 % higher in comparison to that of the fibre laser treated surface. This was by softening of the near surface layer of the Si3N4 which comprised of lower in hardness, which in turn increased the crack resistance. The effects were not similar with the ZrO2 ceramic to that of the Si3N4 as the fibre laser radiation in this case had produced a rise of 34% compared to that of the CO2 laser radiation. This occurred due to propagation of lower crack resulting from the Vickers indentation test during the fibre laser surface treatment which inherently affected the end K1C though an induced compressive stress layer. The K1C modification of the two ceramics treated by the CO2 and the fibre laser was also believed to be influenced by the different laser wavelength and its absorption co-efficient, the beam delivery system as well as the differences in the brightness of the two lasers used.
机译:通过CO2和纤维激光表面处理的方法研究了Si3N4和ZrO2工程陶瓷的断裂韧性(K1c)。通过采用维氏压痕法研究了近表面硬度的变化。然后使用光学仪器测量裂纹长度和几何形状。使用坐标测量机调查金刚石压痕并测量裂纹的长度。此后,采用计算和分析方法确定K1C。与按原样的表面相比,通过二氧化碳和光纤激光器的表面处理发现两种陶瓷的K1C均增加。 Si3N4的CO2激光辐射表面的K1C比经光纤激光处理的表面的K1C高3%以上。这是由于软化了硬度较低的Si3N4的近表层,从而提高了抗裂性。 ZrO2陶瓷的效果与Si3N4的效果不同,因为在这种情况下,光纤激光辐射比CO2激光辐射提高了34%。这是由于在光纤激光表面处理过程中通过维氏压痕测试而产生的较低裂纹的传播,该裂纹通过感应的压应力层固有地影响了端K1C。据信,用二氧化碳和光纤激光器处理的两种陶瓷的K1C改性也受不同的激光波长及其吸收系数,光束传输系统以及所用两种激光器的亮度差异的影响。

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